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Scholars Journal of Applied Medical Sciences | Volume-10 | Issue-03
Synthesis of Antimony Selenide (Sb2Se3) by Wet Milling: Structural Properties
A. A Sifawa, S. Abdullahi, Mamuda. A Sifawa
Published: March 22, 2022 |
148
98
DOI: 10.36347/sjams.2022.v10i03.009
Pages: 327-330
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Abstract
Single-phase bulk Sb2Se3 compound was synthesized by mechanical alloying using elemental precursors, Sb and Se. The collected sample has been successfully characterized by X-Ray diffraction for the wet mill to investigate the formation of Sb2Se3 phase. The XRD results analysis found that Sb2Se3 single phase was formed in 13 hours of milling. Raman shifts of 188 and 252cm-1 for wet as-milled Sb2Se3 had been recorded. EDS exhibits two strong peaks confirming the purity of our sample by detecting only Sb and Se elements, respectively.